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The award-winning Phase Change Matters blog tracks the latest news and research on phase change materials and thermal energy storage. E-mail tips and comments to Ben Welter, communications director at Entropy Solutions. Follow the blog on Twitter at @PureTemp. Subscribe to the weekly PCM newsletter. Or join the discussion on LinkedIn.

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Research roundup: Heat transfer enhancement of PCMs; CuO/palmitic acid composite; cooking applications; more

Ben Welter - Tuesday, June 12, 2018

From Materials Today: Proceedings:

Investigation of thermal performance by applying a solar chimney with PCM towards the natural ventilation of model house under Climate of Thailand
Study of Solar– PCM Walls for domestic hot water production under the tropical climate of Thailand
Improved Performance of Composite Phase Change Material for Thermal Energy Storage
Experimental investigation on freezing/melting characteristics of two different phase change materials
Review on Heat Transfer Enhancement of Phase Change Materials (PCMs)
Experimental Investigation of Improved Thermal Characteristics of Al2O3/Barium Hydroxide Octa Hydrate as Phase Change Materials (PCMs)
Improved Thermal Energy Storage Behavior of CuO/Palmitic acid Composite as Phase Change Material

From Applied Thermal Engineering:

An Experimental Investigation of the Melting Process of a Bio-based Nano-PCM filled Vertical Cylindrical Thermal Energy Storage System

From International Journal of Heat and Mass Transfer:

Experimental investigation of the effects of mass fraction and temperature on the viscosity of microencapsulated PCM slurry

From Journal of the Brazilian Society of Mechanical Sciences and Engineering:

Rapid thermal cycling of three phase change materials (PCMs) for cooking applications

From 3rd Thermal and Fluids Engineering Conference:

Use of Wood/Phase Change Material Composite in the Building Envelope for Building Thermal Control and Energy Savings

Research roundup: Thermoelectric generator system; solar chimney; novel thermal management system for lithium-ion battery pack; more

Ben Welter - Friday, May 18, 2018

From Energy:

Protection and Thermal Management of Thermoelectric Generator System Using Phase Change Materials: An Experimental Investigation
Performance analysis of a novel thermal management system with composite phase change material for a lithium-ion battery pack

From Solar Energy:

Efficient energy storage technologies for photovoltaic systems
The experimental appraisement of the effect of energy storage on the performance of solar chimney using phase change material

From Applied Thermal Engineering:

Improving thermal management of electronic apparatus with paraffin (PA)/expanded graphite (EG)/graphene (GN) composite material
Experimental exploration of incorporating form-stable hydrate salt phase change materials into cement mortar for thermal energy storage

From Thermal Science and Engineering Progress:

Role of Metallic Foam in Heat Storage in the Presence of Nanofluid and MicroEncapsulated Phase Change Material

From International Journal of Heat and Mass Transfer:

Numerical investigation of thermal and optical performance of window units filled with nanoparticle enhanced PCM

From Applied Energy:

Cost estimation and sensitivity analysis of a latent thermal energy storage system for supplementary cooling of air cooled condensers
Influence of design on performance of a latent heat storage system at high temperatures

From Energy Conversion and Management:

Preparation and investigation of distinct and shape stable paraffin/SiO2 composite PCM nanospheres

From Energy and Buildings:

Parametric Analysis of Using PCM Walls for Heating Loads Reduction

PCM briefing: BASF to spend $2.2 billion on R&D; Sunamp heat batteries qualify for Scottish loan program

Ben Welter - Monday, May 14, 2018

Chemical & Engineering News reports that the top 50 U.S. chemical producers generated $285.4 billion in chemical revenues in 2017, a 9.4 percent increase over 2016. 

• Under its new CEO, Martin Brüdermüller, BASF is planning to pour $2.2 billion into research and development, making BASF the second-highest investor in innovation in the chemicals sector after DuPont

Grace HsiaWarmilu LLC founder Grace Hsia, right, is on Crain's 20 in Their 20s list honoring Michigan's rising young leaders. Warmilu makes a PCM-equipped infant warming blanket.   

Axiom Exergy of Richmond, Calif., has raised $7.6 million in Series A funding, for a total of $12.5 million raised to date. The round was co-led by GXP Investments and Shell Ventures. Axiom's PCM-based "refrigeration battery" is designed to reduce energy supermarket energy costs. 

Sunamp Ltd. is applauding the Scottish government's decision to include heat batteries to its Home Energy Scotland Loan program. Homeowners and private landlords are now eligible to apply for an interest-free loan of up to 6,000 pounds to install Sunamp's PCM-based heat battery systems.

• Albuquerque-based SAVSU Technologies is launching two new high-performance shipping containers branded as Evo Extreme. The containers are designed for the 2-8C and -80C temperature ranges.

Emirates District Cooling has won a contract to supply a district cooling system to the Expo Dubai 2020 event. The system will have a capacity of 60,000 tons of refrigeration. 

• Georg Rodriguez, managing director at MUTZ Engineering mbH, will present a free lecture, presumably in German, on "phase change materials for temperature management and energy storage in buildings" on Tuesday, May 15, at the KEBAB lecture room in Berlin.

Patent application: Pasteurization for small containers using a PCM

Ben Welter - Thursday, April 05, 2018

U.S. patent application 20180092371 (inventors Micaela Langille Collins and Yu-ling Cheng, Toronto, Canada; Scott Nicholas Genin, Unionville, Canada; and Jayesh Kumar Srivastava, West Toronto, Canada):

"A pasteurization device comprising an insulated heating tub, a metal grid heat sink, 69° C. melt-point paraffin wax, wherein the metal grid heat sink and the paraffin wax are combined inside the insulated heating tub; a temperature sensor connected to a microprocessor controlled device, suitable to measure temperature and to generate an alarm, a top plate, and a material suitable to cover the wax; wherein the top plate comprises a plurality of openings corresponding to an opening in the metal grid heat sink of suitable size to accept a baby bottle; wherein the insulated heating tub can be heated to at least 73° C. and wherein the microprocessor controlled device provides an audible tone upon the temperature sensor reading 73° C. for at least 30 seconds."

http://www.freepatentsonline.com/20180092371.pdf

So, which PCM product idea was phony?

Ben Welter - Monday, January 08, 2018

In 2017's final issue of Phase Change Matters, we challenged readers to identify which of these PCM product ideas was phony: an edible additive for chocolate, a feminine pad with cooling properties, a cooling pad for chickens, a thermally responsive bra and a temperature-controlled shipping container for mosquito eggs. 

It was a trick question: All five product ideas were serious inquiries submitted to Entropy Solutions in the past year. Thanks to Holger Böhme, Shaun Mann and Kosheela Poo Palam for submitting answers - and for subscribing to our newsletter. Each will receive a PureTemp temperature-control coffee tumbler.

Which PCM product idea is phony? Answer correctly for a chance to win a PureTemp mug

Ben Welter - Tuesday, January 02, 2018

PureTemp tumbler Entropy Solutions receives a dozen or so inquiries each week, most of them serious questions about PCM products, pricing and suitability for various applications. But some inquiries stretch the bounds of believability. Can you identify which of the product ideas below is fake? 

Send your answer to bwelter@puretemp.com. Five winners will be randomly selected from correct entries received by Jan. 4. The prize: a prototype coffee tumbler developed by Entropy Solutions several years ago, a product idea that was totally legit.

NOTE: You must be a Phase Change Matters subscriber to submit an entry. Representatives of organizations attending the first meeting of the PCM Industry Association of North America in October know the answer and are not eligible for this contest. Good luck to all the contestants!

Chocolate1. Mmm chocolate

We are exploring new ingredient technologies to produce a chocolate product that will release heat when it is consumed. Standard chocolate produces a minor cooling effect when it's melting in the mouth – the main fat is cocoa butter. The idea is to develop a new filling fat/oil that will release heat when consumed.

2. Premium padsWonder Woman

I represent a consumer goods company that is seeking materials that could help the feminine pad feel ‘cool’ in order to increase the comfort of use, especially when female is engaging in activities such as boxing, distance running and other extreme athletic challenges.

Chickens3. Chicken helper

I am hoping phase change materials could help solve a problem I have. First, I am completely serious. Second, here is the problem: I live in Texas and have 10 back yard laying hens. It is hot. Chickens start to go into heat stress at 85 degrees. Is it possible to enclose PCMs into a sort of pad for my chickens to rest near during the day?

Golden Girls4. Hot flashes

I am interested in using your product for a product I am developing for my design thesis. I am trying to make a responsive bra that senses a hot flash, and responds by turning on peltiers and "conducting" the cold through some sort of gel medium to the skin. Are any of your products the right thing for this?

Mosquito eggs5. Mosquito eggs

I'm wanting to ship mosquito eggs and need the parcel to stay dry, and within a prescribed temperature range of 10-35 degrees for up to three days. Would you be able to recommend a particular product of yours which could meet these requirements?

PCM briefing: Registration open for PCM 2018 in Quebec; MIT finds new way to mix oil, water

Ben Welter - Friday, November 10, 2017

• Registration is open for PCM 2018, the 12th IIR Conference on Phase Change Materials and Slurries for Refrigeration and Air Conditioning. The conference will be held May 21-23, 2018, in Orford, Québec. Topics will include thermal energy storage; thermophysical and rheological properties of PCMs and slurries; and transport phenomena and time-dependent behavior of PCMs and slurries.

MIT researchers have developed a new way to mix oil and water and create an emulsion that remains stable for long periods — no shaking required.

• Registration is open for "Towards a Sustainable Solution to Melt Snow and Ice on Concrete Pavement: Use of Phase Change Materials, a presentation by Dr. Yaghoob Farnam, an assistant professor in the Department of Civil, Architectural and Environmental Engineering at Drexel University. Farnam will discuss his research on the use of PCM-enhanced concrete to inhibit the buildup of snow and ice on pavement. The program will be held Nov. 30 in King of Prussia, Penn.

• "Innovative Thoughts" blogger Harvey Wade visited the 3M Customer Innovation Centre in Bracknell, U.K., last month to find out how the big company sustains its innovative edge. Lesson No. 1: 3M listens to its customers. "They don’t guess what the customer needs," Wade writes, "they invest their time to know their needs, discovering the big problems that they can try to solve." 

BMW PCM Ride jacketBMW's 2018 Motorrad collection includes the latest version of the PCM Ride jacket, featuring microencapsulated phase change material that "adapts permanently and smartly to the current temperature."

Peli BioThermal has opened a service center in Brussels, Belgium, to handle its Credo line of reusable temperature-controlled packaging. 

Ember Technologies' newest temperature-control product, a $79 ceramic mug with an active heating system, contains no phase change material. The company's first product, a PCM-lined travel tumbler, sells for $150.

Grace Hsia, founder and CEO of Warmilu, a Michigan startup that makes an infant warming blanket, talks about the stresses and rewards of building a company from scratch. "I find my body will sometimes crash," Hsia told Crain's Detroit Business, explaining how 90-hour workweeks have led to bouts of pneumonia and bronchitis. "I've been trying to get more sleep, which is tough."

The preliminary program has been released for the fifth Building Enclosure Science & Technology conference, known as BEST5. It will take place April 15-18 in Philadelphia. 

• The American Chemical Society has won its lawsuit against Sci-Hub, a widely used pirate site for scientific papers that was established in 2011 by former neuroscientist Alexandra Elbakyan.

• New from Intellectual Research Partners: "Global Thermal Energy Storage (TES) systems Market By Technology (Molten salt, Phase change materials, Water based, Electric thermal and Solar) End User Application (Air Conditioning, Cold Storage, Power Storage, Process Cooling) Region (North America, Europe, APAC) Forecast To 2023"

Patent application: Heat retaining dish assembly

Ben Welter - Friday, October 27, 2017

Patent application 20170303710 (applicant Tempra Technology Inc., Bradenton, Fla.):

"A dish assembly for serving food includes a dish housing that defines a surface, upon which the food can be placed, and an inner compartment, a phase-change material within the inner compartment, and an electrically-conductive element inside the inner compartment and thermally coupled to the phase-change material. In a typical implementation, the phase-change material is adapted to melt in response to the electrically-conductive element being heated by an electromagnetic induction heater. The thus heated dish assembly can facilitate getting hot food to a table while it is still hot, and once at the table, keeping that hot food at least warm for quite some time, while it is consumed."

http://www.freepatentsonline.com/20170303710.pdf

Patent application: Product transport container

Ben Welter - Wednesday, September 13, 2017

U.S. patent application 20170253409 (applicant Phase Change Energy Solutions Inc., Asheboro, N.C.):

PCES patent drawing"Product transport containers are disclosed. Such containers can provide one or more advantages compared to existing containers. For example, product transport containers described herein can maintain a product at a desired temperature for an extended period of time, including without the use of an active heating or cooling component. Such product transport containers described herein may also provide improved breathability, thermal insulation, and/or mechanical strength or dimensional stability. Such containers can include a plurality of walls defining an interior volume and a selectively openable side permitting movement of the product into and out of the interior volume of the container. The walls can be formed from a thermoformed non-woven fabric."

http://www.freepatentsonline.com/20170253409.pdf

Smart pet feeder keeps Fido's kibble cool with PCM

Ben Welter - Thursday, September 07, 2017

It's not much to look at, but an ingenious assembly of off-the-shelf electronic components could be just what a busy (and geeky) pet owner needs. The Mario Feeder allows users to schedule and monitor pet feedings from a smart phone and plays a personalized message alerting Fido when it's time to chow down. If Fido fails to heed the call, an alert will be sent to the owner's phone. Other features of the rotating dispenser include:

Mario FeederProximity detection: The bowl will open only when your RFID-tagged pet is nearby, to stop other animals from stealing food.

Bark detection: The feeder is "constantly listening" and will send an alert if your pet sounds distressed.

Smart scale: Tracks what your pet eats, when it eats and how much it eats.

Phase change material: Keeps perishable food cold. 

Developers have launched an Indiegogo campaign in hopes of raising $46,500 to help bring the product to market. They've also produced a video that might be the cutest ad you'll see on the Internet today:

Mario pet feeder video grab

Lead engineer Justin O'Neill answered a few PCM-focused questions by e-mail:

Q: What type of PCM is used? 

A: "We believe that the ability to keep food cold throughout the day is an important feature in a premium pet feeder, and strangely absent in competing products. We are using an organic PCM with a melting point of around 6 degrees Celsius. ... [It is] a bio-based PCM. This isn't because we believe there is a risk of food contamination (very small risk since we are using a robust casing) but more of a product life-cycle consideration with disposal."

Q: How is the PCM encapsulated? 

A: "The PCM is encapsulated in the walls and base of the main bowl, and it is recharged by placing the whole bowl into the freezer/ fridge. We did play with the idea of having separate removable compartments, but this did not fit with our ethos of reducing the total number of components. The bowl is sized so that it will fit in to most domestic freezers/ fridges (also less fiddly for the user). ... Our final design has two compartments with thicker base to hold more PCM. Prototypes have been developed with an ABS housing, but the final version could be PP or HDPE. ... We would have loved to use aluminium or stainless casing but the bowl is a fairly complex moulding and I suspect we would have ended up with high pressure die casting and a step change in cost."

Q: What are the dimensions of the product? 

A: "The bowl is ~310mm in diameter, depending on where exactly you are measuring. We tried to balance catering to larger pets with ensuring it isn't too big for apartments, and of course getting the food bowl with PCM it into a fridge/ freezer."

Q: How long does the product provide a cooling effect?

A: "Our intent is only to provide the ability to delay food spoiling, not keep it frozen or cold indefinitely. Our target has been delaying spoiling for 3-4 hours vs food being exposed, and obviously the performance varies greatly with ambient temperature, the foodstuff and volume of food. The Mario feeder allows users to set an expiration time. I.e after a specified time a particular compartment will be forbidden to expose even if the dog is near (RFID proximity detection) as food may be spoiled. By keeping food out of the sun (using proximity detection and rotating the bowl) we further improve total performance."