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The award-winning Phase Change Matters blog tracks the latest news and research on phase change materials and thermal energy storage. E-mail tips and comments to Ben Welter, communications director at Entropy Solutions. Follow the blog on Twitter at @PureTemp. Subscribe to the weekly PCM newsletter. Or join the discussion on LinkedIn.

Two Entropy advisors, Dr. Mohammed Farid and Lucas B. Hyman, are pleased to take your questions about PCMs and thermal energy storage. Send your questions to bwelter@puretemp.com. We'll select the best and post the answers here each week.

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Research roundup: Macro-packed fatty acid ester composites; selective laser sintering; more

Ben Welter - Tuesday, July 11, 2017

From Journal of Industrial and Engineering Chemistry:

Performance evaluation of macro-packed fatty acid ester composites using energy-efficient thermal storage systems

From Procedia Manufacturing:

Selective Laser Sintering of Phase Change Materials for Thermal Energy Storage Applications

From Applied Energy:

Synthesis and characterization of microencapsulated myristic acid–palmitic acid eutectic mixture as phase change material for thermal energy storage
Advances in thermal energy storage materials and their applications towards zero energy buildings: A critical review

From Solar Energy Materials and Solar Cells:

A new strategy for enhanced latent heat energy storage with microencapsulated phase change material saturated in metal foam
Preparation and characterization of hybrid nanocomposite embedded organic methyl ester as phase change material

From Renewable Energy:

Cutting copper fiber/paraffin composite phase change material discharging experimental study based on heat dissipation capability of Li-ion battery

From Lehigh University:

Numerical and Experimental Study of the Melting Process of a Phase Change Material in a Partically Filled Spherical Shell [thesis]

From IEEE Internet Computing:

Thermal Time Shifting: Decreasing Datacenter Cooling Costs with Phase Change Materials

From International Journal of Heat and Mass Transfer:

Numerical modeling of solid-liquid phase change in a closed 2D cavity with density change, elastic wall and natural convection

From Applied Thermal Engineering:

Evaluation of the suitability of different calorimetric methods to determine the enthalpy-temperature curve of granular PCM composites
Heat Transfer Enhancement during Freezing Process of Nano Phase Change Material (NPCM) In a Spherical Capsule
Numerical simulation on thermal characteristics of supercooled salt hydrate PCM for energy storage: Multiphase model

Research roundup: INPATH-TES Ph.D. program; waste-to-energy plants; EnergyPlus-based building model; more

Ben Welter - Thursday, June 29, 2017

INPATH-TES: Innovative pathways to PhD research in thermal energy storage [Sustainable and Renewable Energy Engineering]

Application of high temperature phase change materials for improved efficiency in waste-to-energy plants [Waste Management]

Experimental investigation and EnergyPlus-based model prediction of thermal behavior of building containing phase change material [Journal of Building Engineering]

Experimental Analysis of Graphite Dispersed Salt Hydrates based Phase Change Materials to Determine Enhancement in their Thermophysical Properties [pdf] [Journal of Chemical and Pharmaceutical Sciences]

Use of phase change materials during compressed air expansion for isothermal CAES plants [35th UIT Heat Transfer Conference]

Simulation of Melting Process of a Phase Change Material (PCM) using ANSYS (Fluent) [pdf] [International Research Journal of Engineering and Technology]

Cellulose/Paraffin Composite Fibers for Thermal Energy Storage and Temperature Regulation [IUMRS International Conference in Asia]

Enhanced Specific Heat Capacity of Binary Chloride Salt by Dissolving Magnesium for High-temperature Thermal Energy Storage and Transfer [Journal of Materials Chemistry A]

Research roundup: Graphite particle fillers; sodium nitrate microcapsules; domestic space heating in UK; more

Ben Welter - Tuesday, June 27, 2017

Effect of temperature and graphite particle fillers on thermal conductivity and viscosity of phase change material n-eicosane [International Journal of Heat and Mass Transfer]

Thermal stability of sodium nitrate microcapsules for high-temperature thermal energy storage [Solar Energy Materials and Solar Cells]

Phase change materials to meet domestic space heating demand in the UK - A numerical study [Journal of Fluid Flow, Heat and Mass Transfer]

Synthesis of three-dimensional graphene aerogel encapsulating n-octadecane for enhancing phase-change behavior and thermal conductivity [Journal of Materials Chemistry A]

A recyclable thermochromic elastic phase change oleogel for cold compress therapy [Applied Thermal Engineering]

Research roundup: PCM-assisted night purge ventilation; dispersed metallic nanoparticles; crystallohydrates; more

Ben Welter - Tuesday, June 20, 2017

Nanoencapsulated crystallohydrate mixtures for advanced thermal energy storage [Journal of Materials Chemistry A]

Hexadecane-in-water emulsions as thermal-energy storage and heat transfer fluids: Connections between phase-transition temperature and period of hexadecane droplets dispersed in hexadecane-in-water emulsions and characteristics of surfactants [Colloids and Surfaces A: Physicochemical and Engineering Aspects]

Evaluating the Performance of American Change Phase Paraffin Cooling Vest and Iranian Spadana Gel Ice Cooling Vest on the Perceptual and Physiological Strain Score Index in Hot and Humid Working Conditions of Assaluyeh in Iran [International Journal of Occupational Hygiene]

Development of thermal enhanced n-octadecane/porous nano carbon-based materials using 3-step filtered vacuum impregnation method [Thermochimica Acta]

The impact of phase change materials assisted night purge ventilation on the indoor thermal conditions of office buildings in hot-arid climates [Energy and Buildings]

Thermal energy harvest in the discharge of CO2 semi-clathrate hydrate in an emulated cold storage system [Applied Thermal Engineering]

Melting dynamics of a phase change material (PCM) with dispersed metallic nanoparticles using transport coefficients from empirical and mean field models [Applied Thermal Engineering]

Comparative assessment of thermal comfort with insulation and phase change materials utilizations in building roofs and walls [pdf] [Advanced Materials Proceedings]

Fabrication and properties of graphene oxide-grafted-poly(hexadecyl acrylate) as a solid-solid phase change material [Composites Science and Technology]

Patent application: Compressed gas energy storage and harvesting system

Ben Welter - Wednesday, June 14, 2017

U.S. patent application 20170160019 (applicant IFP Energies Nouvelles, France ):

"The present invention relates to an AACAES system and method in which balls make it possible to store heat. The heat exchanges are produced by means of at least one radial heat exchanger, in which the balls and a first fluid circulate, the first fluid passing radially through means for circulating the balls. ... [Said] heat storage balls are produced in alumina, in metal or by micro or nano capsules of phase change material, such as paraffins, metals or salts. "

http://www.freepatentsonline.com/20170160019.pdf

Research roundup: Shape-stabilized PCM in epoxy matrix; myristyl alcohol/metal foam for solar thermal storage; more

Ben Welter - Thursday, June 01, 2017

Illustration of shape-stabilized PCM in epoxy matrix

Novel shape stabilized phase change material based on epoxy matrix with ultrahigh cycle life for thermal energy storage [Applied Thermal Engineering]

Thermal and electrical performance of a PV module integrated with double layers of water-saturated MEPCM [Applied Thermal Engineering]

Investigation on thermal and mechanical characteristics of concrete mixed with shape stabilized phase change material for mix design [Construction and Building Materials]

Thermal properties and thermal conductivity enhancement of composite phase change materials using myristyl alcohol/metal foam for solar thermal storage [Solar Energy Materials and Solar Cells]

Experimental and Numerical Study on Energy Performance of Buildings Integrated with Phase Change Materials [Energy Procedia]

Evaluation on Performance of a Phase Change Material Based Cold Storage House [Energy Procedia]

Using Phase Change Materials to Reduce Overheating Issues in UK Residential Buildings [Energy Procedia]

Effect of Supercooling on the Solidification Process of the Phase Change Material [Energy Procedia]

Experimental Investigation of a Spiral Tube Embedded Latent Thermal Energy Storage Tank Using Paraffin as PCM [Energy Procedia]

Investigation of specific heat and latent heat enhancement in hydrate salt based TiO2 nanofluid phase change material [Applied Thermal Engineering]

Modeling and investigation of high temperature phase change materials (PCM) in different storage tank configurations [Journal of Cleaner Production]

Lauric acid/modified sepiolite composite as a form-stable phase change material for thermal energy storage [Applied Clay Science]

PCM briefing: Outlast introduces Xelerate fabric; Warmilu signs 2 distributors

Ben Welter - Friday, May 19, 2017

Drawing of Outlast Xelerate

Outlast Europe's Martin Bentz spoke with T.EVO magazine this month about the company's new Xelerate fabric. The fabric, introduced at a German trade fair earlier this year, incorporates "heat spreader" technology, a process traditionally known for cooling electronic devices. Xelerate fabric features improved thermal conductivity, Bentz said, and is suitable for home textiles, sportswear and protective gear. In an email exchange with Phase Change Matters, Bentz declined to discuss specific partners or customers.

Warmilu, maker of the IncuBlanket infant warmer, reports that is on track for $300,000 in total 2017 sales after signing two distributors for Latin America, Africa and Southeast Asia: Relief for Africa Foundation and Maternova. The IncuBlanket, which has been successfully tested in clinical trials in India, uses packs filled with sodium acetate trihydrate to keep infants warm for up to five hours. CEO Grace Hsia says the device recently cleared its first regulatory filing with Kenya's Pharmacy and Poisons Board.

Axiom Exergy has won a Gold Stevie for Energy Innovation in the 15th annual American Business Awards. Axiom's "refrigeration battery" enables supermarkets and food warehouses to store thermal energy at night when power is cheaper. The system, which uses salt-based phase change material, reduces peak power usage by up to 40 percent.

• Registration is open for IFAI's Expo 2017, set for Sept. 27-29 in New Orleans. The Industrial Fabrics Association International show will feature sessions on smart fabrics, military procurement, biomimesis and green certification.   

Pelican BioThermal has introduced a new Series 22 Universal system for its Credo brand of shippers. The system uses a dual PCM coolant system designed to be operational throughout the year.

National Law Review offers a fresh overview of green chemistry laws across the United States. "State chemical control regimes," the authors conclude, "are likely to increase cost and foster confusion about chemical safety, which is one reason that Congress agreed to modernize TSCA by adopting LCSA."

Monodraught's Cool-phase ventilation and cooling system was among the finalists honored at the National CSR Awards in London this week. The hybrid system, which won a "One to Watch" award, uses PCMs to store and release thermal energy, providing a free cooling load and reducing energy and maintenance costs.

• The agenda has been released for the 15th Cold Chain Global Forum to be held Sept. 25-29 in Chicago. Frank Butch, director of engineering at Sonoco ThermoSafe, will lead a master class on temperature assurance packaging certification.

Bloomberg BNA is offering a free webinar June 12: "Reviewing New Chemicals under Amended TSCA: Impact on Innovation." 

Outlast Europe's Martin Bentz spoke with T.EVO magazine this month about the company's new Xelerate fabric (shown below). The fabric, introduced at a German trade fair earlier this year, incorporates "heat spreader" technology, a process traditionally known for cooling electronic devices. Xelerate fabric features improved thermal conductivity, Bentz said, and is suitable for home textiles, sportswear and protective gear. In an email exchange with Phase Change Matters, Bentz declined to discuss specific partners or customers.

Research roundup: Crystallization of salt hydrates in polymeric foam; Glauber's salt; cetyl alcohol/HDPE composites; more

Ben Welter - Thursday, May 18, 2017

Numerical study on melt fraction during melting of phase change material inside a sphere [International Journal of Hydrogen Energy]

Crystallization of inorganic salt hydrates in polymeric foam for thermal energy storage application [Journal of Energy Storage]

Evaluating the passive and free cooling application methods of phase change materials in residential buildings: A comparative study [Energy and Buildings]

Microstructure and thermal properties of cetyl alcohol/high density polyethylene composite phase change materials with carbon fiber as shape-stabilized thermal storage materials [Applied Energy]

Screening alternatives for producing paraffinic phase change materials for thermal energy storage in buildings [International Journal of Energy Research]

Various Applications of Phase Change Materials: Thermal Energy Storing Materials [pdf] [International Journal of Emerging Research in Management]

Preparation and thermal properties of Glauber’s salt-based phase-change materials for Qinghai–Tibet Plateau solar greenhouses [International Journal of Modern Physics B]

Numerical analysis on the energy storage efficiency of phase change material embedded in finned metal foam with graded porosity [Applied Thermal Engineering]

Passive cooling potential in buildings under various climatic conditions in India [Renewable and Sustainable Energy Reviews]

BASF sells Micronal PCM line to Microtek Labs

Ben Welter - Wednesday, May 17, 2017

Microtek Laboratories of Dayton, Ohio, today announced it has signed a contract to purchase BASF's Micronal line of microencapsulated phase change material. Financial terms of the deal were not disclosed.

Micronal logoThe Micronal line, introduced in 2004, includes six paraffin-based PCMs offered in liquid and powder form, with melt points ranging from 21° C to 26° C. Microencapsulated PCMs are used for thermal regulation in building and construction products, mattresses, textiles and packaging applications. Micronal is key component of building products such as Knauf wallboard and National Gypsum's ThermalCORE panels. 

Manufacturing of Micronal products will be transitioned to Microtek’s Dayton production facility by the end of the year. Microtek has taken ownership of all Micronal inventory and will begin working with Micronal customers on May 23.

“This is great addition to Microtek’s product line, creating a real advantage for customers who already have a defined manufacturing/coating process requiring a specific type of phase change product in their formulation,” said Randall Lane, Microtek’s chief strategy officer. “Microtek’s mission has always been to provide innovative solutions to enhance product performance for our customers. Adding Micronal to the product line allows Microtek to remain the world leader in microencapsulated PCM products.”

BASF, based in Ludwigshafen, Germany, said the sale will allow its dispersions and pigments division to focus on its core business, "dispersions and additives in the field of raw materials used in construction chemicals." BASF said the sale does not include Ludwigshafen production assets or employees.

Microtek, founded in 1985, is a privately held company focused on phase change material and microencapsulation services. It introduced its Nextek line of PCM capsules in 2016.

https://www.basf.com/en/company/news-and-media/news-releases/2017/05/p-17-225.html

http://www.businesswire.com/news/home/20170517005136/en/Microtek-Laboratories-Announces-Acquisition-Micronal-Product-Line

Research roundup: Expanded graphite/adipic acid composite PCMs; nanomagnetite enhanced paraffin; more

Ben Welter - Friday, April 28, 2017

From Journal of Thermal Analysis and Calorimetry:

Preparation and thermal cycling of expanded graphite/adipic acid composite phase change materials

From RSC Advances:

Phase change materials of fatty amine-modified silicate clays of nano layered structures
Myristic acid-hybridized diatomite composite as a shape-stabilized phase change material for thermal energy storage

From 4th Sustainable Thermal Energy Management International Conference:

Domestic thermal storage requirements for heat demand flexibility

From Smart Materials and Nondestructive Evaluation for Energy Systems:

Novel dynamic thermal characterization of multifunctional concretes with microencapsulated phase change materials

From Digest Journal of Nanomaterials and Biostructures:

Nanomagnetite Enhanced Paraffin for Thermal Energy Storage Applications [pdf]

From Energy Procedia:

Solar Thermal Energy with Molten-salt Storage for Residential Heating Application

From Solar Energy:

Performance study and analysis of an inclined concentrated photovoltaic-phase change material system

From Energy:

Preparation, thermal properties and thermal reliability of a novel mid-temperature composite phase change material for energy conservation

From Applied Thermal Engineering:

Investigation on the thermal performance of a high-temperature latent heat storage system

From Cement and Concrete Composites:

Numerical simulations to quantify the influence of Phase Change Materials (PCMs) on the early- and later-age thermal response of concrete pavements

From International Journal of Refrigeration:

Performance study on air-cooled household refrigerator with cold storage phase change materials

From Energy and Buildings:

Novel thermosetting phase change materials with polycarbonatediol based curing agent as supporting skeleton for thermal energy storage 

From Journal of Cleaner Production:

Improving thermal response of lightweight timber building envelopes during cooling season in three European locations