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The award-winning Phase Change Matters blog tracks the latest news and research on phase change materials and thermal energy storage. E-mail tips and comments to Ben Welter, communications director at Entropy Solutions. Follow the blog on Twitter at @PureTemp. Subscribe to the weekly PCM newsletter. Or join the discussion on LinkedIn.

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PCM briefing: DowDuPont shifts to small-scale R&D projects; Viking Cold Solutions has opening for business development manager

Ben Welter - Monday, June 04, 2018

Arktek vaccine carrierWired takes a close look at Arktek, "the Ebola vaccine's high-tech thermos." The World Health Organization is using the PCM-equipped container to transport the temperature-sensitive vaccine to wherever it's needed, whatever the conditions. The container is designed keep payloads colder than -65 C for five days.

• With an eye toward increased profits, CEO Edward Breen says DowDuPont is moving away from large-scale R&D projects in favor of less risky initiatives of $30 million or less.

Viking Cold Solutions has posted an opening for a business development manager for the Northeastern United States.

ASHRAE has published a new standard describing a methodology to apply building energy modeling throughout the design process. ASHRAE Standard 209-2018 defines minimum requirements for providing energy design assistance using building energy simulation and analysis.

Pelican BioThermal is opening its first Canadian drop point for the Credo on Demand rental program. The new drop point, at ATS Healthcare headquarters in Toronto, offers customers an additional location to return temperature-control pallet and bulk shippers. 

Research roundup: Nanofluid-based PCMs; microencapsulation of n-alkanes; finned solar PV PCM; more

Ben Welter - Thursday, May 31, 2018

From Chemical Engineering Journal:

Glycolysis of Advanced Polyurethanes Composites containing Thermoregulating Microcapsules

From Applied Thermal Engineering:
From Applied Energy:

From International Journal of Thermal Sciences:

From Chemical Engineering Science:

Research roundup: Thermoelectric generator system; solar chimney; novel thermal management system for lithium-ion battery pack; more

Ben Welter - Friday, May 18, 2018

From Energy:

Protection and Thermal Management of Thermoelectric Generator System Using Phase Change Materials: An Experimental Investigation
Performance analysis of a novel thermal management system with composite phase change material for a lithium-ion battery pack

From Solar Energy:

Efficient energy storage technologies for photovoltaic systems
The experimental appraisement of the effect of energy storage on the performance of solar chimney using phase change material

From Applied Thermal Engineering:

Improving thermal management of electronic apparatus with paraffin (PA)/expanded graphite (EG)/graphene (GN) composite material
Experimental exploration of incorporating form-stable hydrate salt phase change materials into cement mortar for thermal energy storage

From Thermal Science and Engineering Progress:

Role of Metallic Foam in Heat Storage in the Presence of Nanofluid and MicroEncapsulated Phase Change Material

From International Journal of Heat and Mass Transfer:

Numerical investigation of thermal and optical performance of window units filled with nanoparticle enhanced PCM

From Applied Energy:

Cost estimation and sensitivity analysis of a latent thermal energy storage system for supplementary cooling of air cooled condensers
Influence of design on performance of a latent heat storage system at high temperatures

From Energy Conversion and Management:

Preparation and investigation of distinct and shape stable paraffin/SiO2 composite PCM nanospheres

From Energy and Buildings:

Parametric Analysis of Using PCM Walls for Heating Loads Reduction

PCM keeps Embry-Riddle’s EcoCAR entry running cool

Ben Welter - Monday, April 30, 2018

Batteries used in hybrid and electric cars work hard and run hot. Traditional cooling systems use an array of pumps, heat exchangers, cooling fans and hoses to manage that heat. Florida’s Embry-Riddle Aeronautical University needed something lighter and simpler for its entry in the Department of Energy’s EcoCAR 3 competition.

The solution: an aluminum cooling plate filled with biobased phase change material.

A team of mechanical engineering students at the school designed and built the plate under the direction of Sandra Boetcher, associate professor of mechanical engineering.

The school’s EcoCAR entry required that the plate use a PCM with a peak melting point of 45 degrees Celsius (113 degrees F). To achieve that temperature, the team selected two commercially available PCMs – PureTemp 37 and PureTemp 48 – and mixed them together.

Embry-Riddle cold plateBoetcher explains the photo at right:

“That’s the inside of the plate before we sealed the aluminum lid on it. On the inside is a copper tube. At the time we put this in the car, we were under a strict deadline and did not have time to redo the bending of the copper tube. The copper tube feeds a cold ethylene-glycol/water mixture as backup for when the PCM has completely melted and needs to resolidify while the car is driving.

“I was concerned that the copper tube didn’t provide enough coverage of the area, but that cold plate has been in the car for the past 2.5 years and it works great. Actually, the back-up pump that runs the ethylene-glycol/water through the copper tube rarely even turns on which means that under our test-driving conditions, the cold plate is acting 100 percent passive. The terrible part of the PCM is that it loves to leak. We feel that there has been some leaking.”

The plate is lighter and simpler than a water-cooled system. “It doesn’t take any energy to run,” said Patrick Currier, an associate professor who advises the EcoCAR team. “We’re not wasting power cooling things. This is a totally passive system, so unless it leaks, it can’t fail.”

Embry-Riddle filed for a U.S. patent on the device in 2015.

“The diagrams in the patent are similar to what we have in the EcoCAR right now, although the geometry is a little different,” Boetcher said. “The research we are conducting is still on-going. The applications we envision could be anything that requires PCM – battery cooling, building technologies, etc.”

Embry-Riddle is one of 16 North American universities challenged to redesign a 2016 Chevrolet Camaro into a hybrid-electric car to reduce environmental impact, while maintaining the “muscle and performance” the car is known for. 

The teams have had four years to develop their entries. The cars will be put to the test in a variety of events in Arizona and California in May. Winners will be chosen in 40-plus categories at an awards ceremony in Hollywood on May 22, with more than $100,000 in prize money at stake.

Embry-Riddle EcoCAR entry

https://news.erau.edu/headlines/shape-shifters-lightweight-technology-keeps-batteries-cool-supporting-eco-vehicles

Contributions sought for new database on thermal storage materials

Ben Welter - Monday, April 16, 2018

A new database for thermal energy storage materials is being developed within the framework of the International Energy Agency’s Energy Conservation through Energy Storage group, Annex 29 and SHC Task 42.

The database is designed to provide characteristic data for phase change, sorption and thermochemical materials. The website, www.thermalmaterials.org, also offers a wiki with definitions related to thermal energy storage. Both areas are open for contributions.

The phase transition data provided for PCMs must be measured according to a DSC-measurement standard. To ensure the quality of the submitted data, contributors must provide a reference measurement using a PCM provided by Fraunhofer ISE.

Stefan Gschwander, head of Group Heat and Cold Storage at Fraunhofer ISE in Freiburg, Germany, said all submitted data will undergo a review process. “If the data is in line with our requirements it can be published in the public area,” he said.

So far, 15 PCMs are listed in the public area. A restricted area of the database is limited to  independently measured materials.

“The data stored is high-quality data which can be used for research, for example
simulation or to design a system,” Gschwander said. “So for our database, the manufacturers normally do not provide data but sample material that is measured from the institutions that are able to measure according the definitions. So far we have measured PCM from Rubitherm, Sasol and BASF. …

“So far we have about 20 different materials in the restricted area and, as we have used it for the development of the measurement standard, many of the materials have been measured several times by different laboratories so that we have a lot more measurements stored in the database.”

Fraunhofer ISE offers independent characterization of PCM, with fees depending on the material and the DSC required to do the measurement.

The ECES is a technology collaboration group that supports the development of electrical energy storage, thermal energy storage, distributed energy storage and borehole thermal energy storage. For more information on the material database project and characterization services, contact Gschwander at stefan.gschwander@ise.fraunhofer.de.

Research roundup: Biomass carbon aerogels from succulents; novel hybrid cooling for lithium-ion batteries; calcium carbonate, graphene oxide shell; more

Ben Welter - Thursday, March 08, 2018

Leakage-proof Phase Change Composites Supported by Biomass Carbon Aerogels from Succulents [Green Chemistry]

Experimental Investigation of a Novel Hybrid Cooling Method for Lithium-ion Batteries [Applied Thermal Engineering]

Modified phase change microcapsules with calcium carbonate and graphene oxide shell for enhanced energy storage and leakage prevention [Sustainable Chemistry & Engineering]

A Novel Thermal Energy Storage System in Smart Building Based on Phase Change Material [IEEE Transactions on Smart Grid]

Study of Material Compatibility for a Thermal Energy Storage System with Phase Change Material [Energies]

Is a self-sufficient building energy efficient? Lesson learned from a case study in Mediterranean climate [Applied Energy]

For Melbourne family, PCM ceiling mats ‘worth the investment’

Ben Welter - Monday, March 05, 2018

A recent two-story addition to a bungalow in suburban Melbourne, Australia, uses bio-based phase change material as a lightweight alternative to thermal mass.

Interior of Playtime HousePhase Change Energy Solutions BioPCM mats containing about 270 kilograms of phase change material were installed above the ceilings, according to architect Penny Guild of Guild Architects. The PCM has a melting point of 24 degrees C. In an e-mail interview, Guild talked about PCM use in the Playtime House project.

Q: What are the projected energy savings related to PCM use in this project?

A: “We didn’t do any specific calculations, but the manufacturer claims between 40 to 80 percent saving in energy bills. The amount of PCM that was put in the project equates to 10kw hours.”

Q: Have you worked with PCM products in the past? Are there plans to use PCM in future projects?

A: “It’s relatively new for the residential market in Australia so I haven’t used it before. The upfront costs are reasonably high, and being a new product there’s not many people that potential clients can turn for advice on its effectiveness. They can’t just ask a friend ‘did you think the PCM was good value in your house’ because no one else has used it. The clients on this project had a high degree of environmental consciousness and both had a science background of some sort (doctor and teacher) and they felt confidant enough it was worth the investment. As the project was an extension above an existing structure adding traditional heavy mass materials was basically impossible which is where the PCM came in.”

http://www.guildarchitects.com.au/northcote-house/

http://futurist--architecture.blogspot.no/2018/01/playtime-house-in-northcote.html

Research roundup: Enhanced bulk-organic PCMs; cementitious composites; business clothing incorporating PCMs; more

Ben Welter - Wednesday, February 21, 2018

New formulation and characterization of enhanced bulk-organic phase change materials [Energy and Buildings]

Numerical analysis of the freeze-thaw performance of cementitious composites that contain phase change material (PCM) [Materials & Design]

Thermal Properties of Lauric Acid Filled in Carbon Nanotubes as Shape-stabilized Phase Change Materials [Physical Chemistry Chemical Physics]

Thermo-physiological comfort of business clothing incorporating phase change materials in a cold environment [International Journal of Clothing Science and Technology]

Phase change material thermal energy storage for a large scale ammonia chiller/heat pump system [International Institute of Refrigeration]

Case Study of Load Shifting Using Thermal Energy Ice Storage in Public Facilities [Journal of Facility Management]

Microencapsulated phase change materials with composite titania-polyurea (TiO2-PUA) shell [Applied Energy]

Numerical study on the effects of fins and nanoparticles in a shell and tube phase change thermal energy storage unit [Applied Energy]

Research roundup: Acrylic PCM microcapsules; paraffin-water nanoemulsion; two-tank molten salt TES; more

Ben Welter - Wednesday, February 14, 2018

Non-linear system identification of a latent heat thermal energy storage system [Applied Thermal Engineering]

Tailoring of bifunctional microencapsulated phase change materials with CdS/SiO2 double-layered shell for solar photocatalysis and solar thermal energy storage [Applied Thermal Engineering]

Preparation of acrylic PCM microcapsules with dual responsivity to temperature and magnetic field changes [European Polymer Journal]

Paraffin wax–water nanoemulsion: A superior thermal energy storage medium providing higher rate of thermal energy storage per unit heat exchanger volume than water and paraffin wax [Energy Conversion and Management]

Preparation and characterization of stearic acid/polyurethane composites as dual phase change material for thermal energy storage [Journal of Thermal Analysis and Calorimetry]

Efficiency analyses of high temperature thermal energy storage systems of rocks only and rock-PCM capsule combination [Solar Energy]

Thermal performance analysis of PCM wallboards for building application based on numerical simulation [Solar Energy]

Thermal energy storage in district heating: Centralised storage vs. storage in thermal inertia of buildings [Energy Conversion and Management]

Two-tank molten salts thermal energy storage system for solar power plants at pilot plant scale: lessons learnt and recommendations for its design, start-up and operation [Renewable Energy]

PCM briefing: Croda merger talks reported; RAL PCM members to meet March 1

Ben Welter - Monday, February 12, 2018

• British specialty chemicals maker Croda International Plc has held unsuccessful talks with Ashland Global Holdings Inc. about a possible merger, a source familiar with the matter told Reuters last week.

Croda recently redesigned the CrodaTherm website, www.crodatherm.com. The new site offers improved navigation and searchability, a wider range of potential PCM applications and profiles of the CrodaTherm technical team. Visitors can register to log in and download datasheets and order samples. "We are excited to launch this new website, making it even easier for our customers to find us and the products they need," said Graeme Tweddle, global managing director for energy technologies at Croda.

• Members of the RAL Quality Association PCM, a European-based organization established in 2004 to develop standards for the phase change material industry, will meet in Düsseldorf, Germany, on March 1. On the agenda: Quality and testing specifications; improvements to the association's website; member content on the BUILD UP Web portal; promotion of PCMs in the European Union, Germany, Netherlands and the United States; and registration of RAL quality marks.   

Sonoco ThermoSafe is accepting registrations for the company's first Leading Minds Seminar, to be held June 6-7 in Philadelphia. Co-hosted by ELPRO, the seminar is a chance for pharmaceutical manufacturers, supply chain partners and government representatives to discuss temperature-assurance packaging and data monitoring in a collaborative environment. Day two includes a visit to ThermoSafe's design and testing lab in Montgomeryville, Penn.

Sonoco is No. 90 on Barron's inaugural list of "The 100 Most Sustainable Companies." 

• A "measurement and verification study" of a Viking Cold Solutions TES system installed in a 320-square-foot walk-in freezer at a supermarket in Fremont, Calif., showed an 18 percent net reduction in energy consumption.   

• The deadline is Monday, Feb. 12, to submit a concept paper for ARPA-E's OPEN 2018 competition. Up to $100 million is available for new projects that "transform the way we generate, store and use energy."

DLR Group, which part of a public-private collaboration working to develop PCM-based cooling and heating methods for Agua Fria Canyon View High School, has been named one of Arizona's "40 Companies to Watch" in 2018 by AZRE magazine. 

• Entries are being accepted for Bio-Based World News' 2018 Innovation Awards. The four categories are product of the year, chemical innovation of the year, best use of alternative feedstocks and industry story of the year. The entry deadline is Feb. 23. Winners will be honored March 20 at the World Bio Markets conference in Amsterdam. 

• Nantucket, Mass., has approved the installation of an Ice Bear thermal storage and air-conditioning unit in a building owned by the town. Last summer, Genbright won a $1.5 million grant from the state to install the units in more than 200 Nantucket homes, with the goal of reducing peak energy demand and staving off the need for a third undersea power cable for the island. But some residents voiced skepticism about the technology, prompting the town board to approve the test installation.

• Shippers have found that cocoa butter can be hard to contain on long ocean voyages. There have been reports of the material leaking out of containers as it changes phase, clogging bilges and generally making a mess. The Cargo Incident Notification System, established in 2011 to share information on all cargo-related incidents, has issued guidelines that recommend the material be shipped in refrigerated containers, particularly when passing through hot climate zones.